Multi-scale characterizations of thermosensitive adhesive resin embedded with bridging materials: Toward forming stable plugging in fractured formations

Authors

  • Youming Lang School of Petroleum Engineering, China University of Petroleum (East China), Qingdao 266580, P. R. China
  • Yingrui Bai School of Petroleum Engineering, China University of Petroleum (East China), Qingdao 266580, P. R. China; State Key Laboratory of Deep Oil and Gas, China University of Petroleum (East China), Qingdao 266580, P. R. China (Email: smart-byron@163.com)
  • Jinsheng Sun School of Petroleum Engineering, China University of Petroleum (East China), Qingdao 266580, P. R. China; State Key Laboratory of Deep Oil and Gas, China University of Petroleum; CNPC Engineering Technology R&D Company Limited, Beijing 102206, P. R. China
  • Huazhou Li School of Mining and Petroleum Engineering, Faculty of Engineering, University of Alberta, Edmonton T6G 1H9, Canada
  • Jingbin Yang State Key Laboratory of Deep Oil and Gas, China University of Petroleum (East China), Qingdao 266580, P. R. China
  • Kaihe Lv School of Petroleum Engineering, China University of Petroleum (East China), Qingdao 266580, P. R. China

Abstract

Lost circulation in fractured formations remains a persistent challenge in drilling operations, causing substantial economic losses and increased operational risk. Conventional granular bridging packs are mechanically fragile and can be destabilized by pressure fluctuations, limiting one-trip plugging efficiency. This study incorporates a thermosensitive adhesive resin into bridging assemblies to enhance plug integrity by promoting interparticle adhesion and particle-wall coupling after thermal activation. Oscillatory temperature-sweep rheometry is used to quantify the temperature-dependent viscoelastic response of resinparticle composites. A wedge-shaped fracture analogue with photoelastic visualization is used to monitor force chain development and uniformity during progressive loading. Discrete element method simulations in Particle Flow Code, using a linear parallelbond contact model, resolve mesoscale load-transfer pathways and isolate the contribution of adhesive interactions. Results indicate that thermosensitive adhesive resin increases assembly coherence, promotes a stable load-bearing skeleton, and suppresses stress localization that typically precedes plugging failure. The strengthening trend is governed by particle rigidity and surface characteristics, yielding consistent load-transfer patterns across experiments and simulations. These findings demonstrate that thermally activated adhesion can transform unconsolidated granular packs into mechanically stable plugging zones, providing a mechanistic basis for designing high-stability lost circulation control systems in fractured formations.

Document Type: Original article

Cited as: Lang, Y., Bai, Y., Sun, J., Li, H., Yang, J., Lv, K. Multi-scale characterizations of thermosensitive adhesive resin embedded with bridging materials: Toward forming stable plugging in fractured formations. Advances in Geo-Energy Research, 2026, 19(2): 166-181. https://doi.org/10.46690/ager.2026.02.05

DOI:

https://doi.org/10.46690/ager.2026.02.05

Keywords:

Thermosensitive adhesive resin, bridging material, interaction mechanism, discrete element simulation, fracture plugging, lost circulation control

References

Abdelaziz, A., Ha, J., Li, M., et al. Understanding hydraulic fracture mechanisms: From the laboratory to numerical modelling. Advances in Geo-Energy Research, 2023, 7(1): 66-68.

Akbar, R., Setiati, R., Maulindani, S., et al. Practical approaches solving the lost circulation problem during drilling operation. International Journal of Application on Sciences, Technology and Engineering, 2023, 1(1): 253-259.

Almohammed, N., Breuer, M. Modeling and simulation of particle-wall adhesion of aerosol particles in particle-laden turbulent flows. International Journal of Multiphase Flow, 2016, 85: 142-156.

Bai, Y., Liu, Y., Sun, J., et al. Plugging mechanism of rigid and flexible composite plugging materials for millimeter-scale fractures. SPE Journal, 2024, 29(4): 1786-1801.

Baldan, A. Adhesion phenomena in bonded joints. International Journal of Adhesion and Adhesives, 2012, 38: 95-116.

Bao, D., Liu, S., Yang, Y., et al. Preparation and performance of high temperature resistant and high strength self-healing lost circulation material in drilling industry. Petroleum Science, 2025, 22(9): 3655-3670.

Blunt, M. J., Sun, S., Boone, M. A., et al. Digital rock physics and fluid flow in the context of the energy transition. Advances in Geo-Energy Research, 2025, 18(3): 299-302.

Chang, C., Lien, H., Lin, J. Determination of reflection photoelasticity fringes analysis with digital image-discrete processing. Measurement, 2008, 41(8): 862-869.

Chu, J., Huang, G., Li, M., et al. A CFD-DEM simulation study on the evolution of the plugging layer during the temporary plugging and diverting fracturing. Fuel, 2026, 405: 136688.

Elkatatny, S., Ahmed, A., Abughaban, M., et al. Deep illustration for loss of circulation while drilling. Arabian Journal for Science and Engineering, 2020, 45(2): 483-499.

Fan, Z., Liu, D., Heynderickx, G., et al. Interface-resolved simulation of droplet-particle interaction dynamics in multi-particle collisions. Physics of Fluids, 2025, 37(4): 043334.

Feng, Y., Gray, K. Modeling lost circulation through drilling-induced fractures. SPE Journal, 2018, 23(1): 205-223.

Gao, Z., He, H., Yang, Z., et al. Improved adhesion of rubber composites by developing environmentally friendly fiber impregnation coatings with good interfacial modulus transition gradients. Progress in Organic Coatings, 2024, 189: 108325.

Guo, K., Kang, Y., Lin, C., et al. A novel experimental study on plugging performance of lost circulation materials for pressure-sensitive fracture. Geoenergy Science and Engineering, 2024, 242: 213214.

Guo, K., Kang, Y., Xu, C., et al. Plugging mode of flaky lost circulation materials within fractures and mechanism to enhance pressure-bearing capacity for the plugging zone. Petroleum Science, 2025, 22(8): 3315-3332.

Han, Z., Yang, X., Ren, N., et al. Dynamic sealing mechanisms of drilling fluid in fractured coalbed methane formations: a coupled CFD-DEM numerical study. Computers and Geotechnics, 2025, 188: 107560.

Hu, Z., Zhang, Y., Wang, J., et al. Experimental study of a circulation agent dynamic plugging for multi-scale natural fractures. Petroleum Science, 2025, 22(9): 3641-3654.

Kan, H., Nakamura, H., Watano, S., et al. Numerical simulation of particle-particle adhesion by dynamic liquid bridge. Chemical Engineering Science, 2015, 138: 607-615.

Kishi, H., Uesawa, K., Matsuda, S., et al. Adhesive strength and mechanisms of epoxy resins toughened with preformed thermoplastic polymer particles. Journal of Adhesion Science and Technology, 2005, 19(15): 1277-1290.

Kumar, R., Kar, K., Dasgupta, K., et al. Static and dynamic mechanical analysis of graphite flake filled phenolic-carbon fabric composites and their correlation with interfacial interaction parameters. Polymer Engineering & Science, 2018, 58(11): 1987-1998.

Kyriazis, A., Kilian, R., Sinapius, M., et al. Tensile strength and structure of the interface between a room-curing epoxy resin and thermoplastic films for the purpose of sensor integration. Polymers, 2021, 13(3): 330.

Lei, S., Sun, J., Bai, Y., et al. Plugging performance and mechanism of temperature-responsive adhesive lost circulation material. Journal of Petroleum Science and Engineering, 2022, 217: 110771.

Li, L., Li, F., Yang, L., Wang, J., et al. A quantitative extraction method of force chains for composite particles in a photoelastic experiment. Chinese Journal of Engineering, 2018, 40(3): 302-312. (in Chinese)

Maggiore, S., Banea, M. D., Stagnaro, P., et al. A review of structural adhesive joints in hybrid joining processes. Polymers, 2021, 13(22): 3961.

Mohajeri, M., Helmons, R., Rhee, C., et al. A hybrid particle-geometric scaling approach for elasto-plastic adhesive DEM contact models. Powder Technology, 2020, 369: 72-87.

Nguyen, K., Mehrabian, A., Bathija, A., et al. Compression of particulate materials in wellbore fractures and enhancement in the wellbore breakdown limit. Journal of Applied Mechanics, 2022, 89(10): 101002.

Nina, L., Marlis, E., Bogna, S. Bond strength between a high-performance thermoplastic and a veneering resin. The Journal of Prosthetic Dentistry, 2020, 124(6): 790-797.

Pu, L., Xu, P., Xu, M., et al. Lost circulation materials for deep and ultra-deep wells: A review. Journal of Petroleum Science and Engineering, 2022, 214: 110404.

Su, X., Lian, Z., Xiong, H., et al. Laboratory study on a new composite plugging material with high bearing strength and high-temperature resistance. Journal of Chemistry, 2019, 2019: 1874617.

Wang, C., Yao, X., Du, T., et al. High-compression-resistant thermosetting resins as plugging materials for oil-based drilling fluids. Recent Patents on Mechanical Engineering, 2026, 19: 1-11.

Wang, G., Huang, Y. Numerical investigation on the fracture-bridging behaviors of irregular non-spherical stiff particulate lost circulation materials in a fractured leakage well section. Geoenergy Science and Engineering, 2023, 223: 211577.

Wang, J., Li, J., Liu, G., et al. Development of a wellbore heat transfer model considering circulation loss. Arabian Journal of Geosciences, 2020, 13(2): 85.

Wang, J., Liang, C., Pang, W. Photoelastic experiment on force chain evolution of particle aggregate under the conditions of biaxially loading and bilaterally flowing. Rock and Soil Mechanics, 2016, 37(11): 3041-3047. (in Chinese)

Wang, X., You, L., Zhu, B., et al. Numerical simulation of bridging ball plugging mechanism in fractured-vuggy carbonate reservoirs. Energies, 2022, 15(19): 7361.

Wei, H., Xia, J., Zhou, W., et al. Adhesion and cohesion of epoxy-based industrial composite coatings. Composites Part B: Engineering, 2020, 193: 108035.

Wu, H., Li, G., Xu, G., et al. Emulsion properties and plugging performances of active crude oil enhanced by amphiphilic Janus nanosheets. Petroleum Science, 2024, 21(6): 4141-4152.

Wu, J., Li, C., Hailatihan, B., et al. Effect of the addition of thermoplastic resin and composite on mechanical and thermal properties of epoxy resin. Polymers, 2022, 14(6): 1087.

Xu, C., Zhong, J., Luo, S., et al. Mechanism and material development of temperature activated bonding plugging for lost circulation control in deep fractured formations. SPE Journal, 2025, 30(10): 6097-6111.

Yan, X., Huo, B., Deng, S., et al. Clarify the effect of fracture propagation on force chains evolution of plugging zone in deep fractured tight gas reservoir based on photoelastic experiment. Geoenergy Science and Engineering, 2024, 233: 212558.

Yan, X., Xu, C., Kang, Y., et al. Mechanical mechanism of meso-structure instability of fracture plugging zone based on the characterization of force chain network. Acta Petrolei Sinica, 2021, 42(6): 765-775. (in Chinese)

Yan, X., Xu, C., Kang, Y., et al. Mesoscopic structure characterization of plugging zone for lost circulation control in fractured reservoirs based on photoelastic experiment. Journal of Natural Gas Science and Engineering, 2020, 79: 103339.

Yang, L., Ma, J., Chang, X., et al. Novel polymeric organic gelator as lost circulation material for oil-based drilling fluids. Geoenergy Science and Engineering, 2023, 231: 212414.

Yao, X., Jian, L., Xu, W., et al. Digital shifting photoelasticity with optical enlarged unwrapping technology for local stress measurement. Optics & Laser Technology, 2005, 37(7): 582-589.

Zang, X., Qiu, Z., Jiang, L., et al. Unravelling fracture plugging behavior of granular temporary plugging agents for a sustainable geothermal development. Fuel, 2025, 387: 134351.

Zeng, X., Duanmu, W., Gao, Z., et al. Research on flexible base discrete adhesion model of SCAPW for blade machining. Journal of Manufacturing Processes, 2024, 118: 173-186.

Zhao, P., Santana, C., Feng, Y., et al. Mitigating lost circulation: A numerical assessment of wellbore strengthening. Journal of Petroleum Science and Engineering, 2017, 157: 657-670.

Zhao, S., Zhu, D., Bai, B., et al. Experimental study of degradable preformed particle gel (DPPG) as temporary plugging agent for carbonate reservoir matrix acidizing to improve oil recovery. Journal of Petroleum Science and Engineering, 2021, 205: 108760.

Zhu, N., Ding, S., Shi, X., et al. Numerical analysis of the connector effect on cuttings bed transportation while Tripping. Geoenergy Science and Engineering, 2023, 227: 211817.

Downloads

Download data is not yet available.

Published

2026-01-23

How to Cite

Lang, Y., Bai, Y., Sun, J., Li, H., Yang, J., & Lv, K. (2026). Multi-scale characterizations of thermosensitive adhesive resin embedded with bridging materials: Toward forming stable plugging in fractured formations. Advances in Geo-Energy Research, 19(2), 166–181. https://doi.org/10.46690/ager.2026.02.05